Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property

AB Rajput; S Hazra; Gerard Fernando; NN Ghosh

doi:10.1080/15533174.2011.591355

Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property

AB Rajput, S Hazra, Gerard Fernando, NN Ghosh

Metallurgy and Materials

Research output: Contribution to journal › Article

9 Citations (Scopus)

Abstract

An ethylenediamine tetraacetic acid (EDTA) precursor-based chemical method has been reported for preparation of single-phase barium hexaferrite nanopowder. Synthesized powders were characterized by thermogravimetric analysis, differential scanning calorimetric analysis, x-ray diffraction, particle size analysis, transmission electron microscopy, and scanning electron microscopy. DC electrical resistivity and magnetic properties of synthesized BaFe12O19 were measured by using a two-probe method and a vibrating sample magnetometer, respectively. This EDTA precursor-based method has the capability of producing nanostructured pure single-phase BaFe12O19 powder at a comparatively lower calcination temperature and offers the potential of a simpler, more cost-effective route than other reported methods.

Original language	English
Pages (from-to)	1114-1121
Number of pages	8
Journal	Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and
Volume	41
Issue number	9
DOIs	https://doi.org/10.1080/15533174.2011.591355
Publication status	Published - 1 Jan 2011

Keywords

x-ray diffraction
magnetic materials
chemical synthesis
magnetic properties

Access to Document

10.1080/15533174.2011.591355

Cite this

Rajput, AB., Hazra, S., Fernando, G., & Ghosh, NN. (2011). Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property. Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and, 41(9), 1114-1121. https://doi.org/10.1080/15533174.2011.591355

@article{c840b117a903405cb4dc8f4cfa1996ff,

title = "Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property",

abstract = "An ethylenediamine tetraacetic acid (EDTA) precursor-based chemical method has been reported for preparation of single-phase barium hexaferrite nanopowder. Synthesized powders were characterized by thermogravimetric analysis, differential scanning calorimetric analysis, x-ray diffraction, particle size analysis, transmission electron microscopy, and scanning electron microscopy. DC electrical resistivity and magnetic properties of synthesized BaFe12O19 were measured by using a two-probe method and a vibrating sample magnetometer, respectively. This EDTA precursor-based method has the capability of producing nanostructured pure single-phase BaFe12O19 powder at a comparatively lower calcination temperature and offers the potential of a simpler, more cost-effective route than other reported methods.",

keywords = "x-ray diffraction, magnetic materials, chemical synthesis, magnetic properties",

author = "AB Rajput and S Hazra and Gerard Fernando and NN Ghosh",

year = "2011",

month = jan,

day = "1",

doi = "10.1080/15533174.2011.591355",

language = "English",

volume = "41",

pages = "1114--1121",

journal = "Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and",

publisher = "Taylor & Francis",

number = "9",

}

Rajput, AB, Hazra, S, Fernando, G & Ghosh, NN 2011, 'Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property', Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and, vol. 41, no. 9, pp. 1114-1121. https://doi.org/10.1080/15533174.2011.591355

Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property. / Rajput, AB; Hazra, S; Fernando, Gerard et al.
In: Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and, Vol. 41, No. 9, 01.01.2011, p. 1114-1121.

Research output: Contribution to journal › Article

TY - JOUR

T1 - Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property

AU - Rajput, AB

AU - Hazra, S

AU - Fernando, Gerard

AU - Ghosh, NN

PY - 2011/1/1

Y1 - 2011/1/1

N2 - An ethylenediamine tetraacetic acid (EDTA) precursor-based chemical method has been reported for preparation of single-phase barium hexaferrite nanopowder. Synthesized powders were characterized by thermogravimetric analysis, differential scanning calorimetric analysis, x-ray diffraction, particle size analysis, transmission electron microscopy, and scanning electron microscopy. DC electrical resistivity and magnetic properties of synthesized BaFe12O19 were measured by using a two-probe method and a vibrating sample magnetometer, respectively. This EDTA precursor-based method has the capability of producing nanostructured pure single-phase BaFe12O19 powder at a comparatively lower calcination temperature and offers the potential of a simpler, more cost-effective route than other reported methods.

AB - An ethylenediamine tetraacetic acid (EDTA) precursor-based chemical method has been reported for preparation of single-phase barium hexaferrite nanopowder. Synthesized powders were characterized by thermogravimetric analysis, differential scanning calorimetric analysis, x-ray diffraction, particle size analysis, transmission electron microscopy, and scanning electron microscopy. DC electrical resistivity and magnetic properties of synthesized BaFe12O19 were measured by using a two-probe method and a vibrating sample magnetometer, respectively. This EDTA precursor-based method has the capability of producing nanostructured pure single-phase BaFe12O19 powder at a comparatively lower calcination temperature and offers the potential of a simpler, more cost-effective route than other reported methods.

KW - x-ray diffraction

KW - magnetic materials

KW - chemical synthesis

KW - magnetic properties

U2 - 10.1080/15533174.2011.591355

DO - 10.1080/15533174.2011.591355

M3 - Article

VL - 41

SP - 1114

EP - 1121

JO - Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and

JF - Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and

IS - 9

ER -

Rajput AB, Hazra S, Fernando G, Ghosh NN. Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property. Synthesis and Reactivity in Inorganic Metal-Organic and Nano-Metal Chemistry (formerly Synthesis and Reactivity in Inorganic and. 2011 Jan 1;41(9):1114-1121. doi: 10.1080/15533174.2011.591355

Synthesis of Single-Phase Barium Hexaferrite Nanopowder via a Novel EDTA Precursor-Based Route and its DC Resistivity and Magnetic Property

Abstract

Keywords

Access to Document

Fingerprint

Cite this