Growth mechanism of subsurface hydrogen cavities in tungsten exposed to low-energy high-flux hydrogen plasma

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Growth mechanism of subsurface hydrogen cavities in tungsten exposed to low-energy high-flux hydrogen plasma. / Chen, Wanqi; Wang, X. Y. ; Chiu, Yu-Lung; Morgan, T.W.; Guo, W.G. ; Li, K.L.; Yuan, Y. ; Xu, B.; Liu, W.

In: Acta Materialia, Vol. 193, 31.07.2020, p. 19-27.

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Chen, Wanqi ; Wang, X. Y. ; Chiu, Yu-Lung ; Morgan, T.W. ; Guo, W.G. ; Li, K.L. ; Yuan, Y. ; Xu, B. ; Liu, W. / Growth mechanism of subsurface hydrogen cavities in tungsten exposed to low-energy high-flux hydrogen plasma. In: Acta Materialia. 2020 ; Vol. 193. pp. 19-27.

Bibtex

@article{e78640c2871846ba8fbc7598f0c32e71,
title = "Growth mechanism of subsurface hydrogen cavities in tungsten exposed to low-energy high-flux hydrogen plasma",
abstract = "Due to a lack of direct experimental results, the detailed mechanisms that govern the blistering behavior of tungsten (W) exposed to ITER-relevant condition in nuclear fusion remain unclear. The growth mechanism of hydrogen (H) blisters is one example. In this work, recrystallized W was exposed to H plasma at 50 eV, 1.5×10 26m −2, and 573 K. Transmission electron microscopy (TEM) samples were prepared using plasma-focused ion beam (FIB) followed by flash-polishing to effectively remove surface damages induced by FIB. The TEM images revealed that the general blisters observed on the exposed surface are associated with underlying cavities. A considerable amount of dislocations were found in the vicinity of the cavities. Prismatic dislocation loop arrays were observed, including small size 'coffee-bean' prismatic loops and large size prismatic loops. Near the tip of surfaces cavities, evidences for the emission of shear loops were also found. Based on the experimental findings, a multi-stage growth mechanism of H cavities was proposed. The loop-punching mechanism is operative for both very small cavities and cavities with sizes larger than several hundreds of nanometers. Whereas at intermediate sizes, cavities grow by emitting shear loops from the cavity tip. ",
keywords = "Blistering behavior, H plasma, Loop punching, Shear loop emission, Tungsten",
author = "Wanqi Chen and Wang, {X. Y.} and Yu-Lung Chiu and T.W. Morgan and W.G. Guo and K.L. Li and Y. Yuan and B. Xu and W. Liu",
year = "2020",
month = jul,
day = "31",
doi = "10.1016/j.actamat.2020.04.012",
language = "English",
volume = "193",
pages = "19--27",
journal = "Acta Materialia",
issn = "1359-6454",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Growth mechanism of subsurface hydrogen cavities in tungsten exposed to low-energy high-flux hydrogen plasma

AU - Chen, Wanqi

AU - Wang, X. Y.

AU - Chiu, Yu-Lung

AU - Morgan, T.W.

AU - Guo, W.G.

AU - Li, K.L.

AU - Yuan, Y.

AU - Xu, B.

AU - Liu, W.

PY - 2020/7/31

Y1 - 2020/7/31

N2 - Due to a lack of direct experimental results, the detailed mechanisms that govern the blistering behavior of tungsten (W) exposed to ITER-relevant condition in nuclear fusion remain unclear. The growth mechanism of hydrogen (H) blisters is one example. In this work, recrystallized W was exposed to H plasma at 50 eV, 1.5×10 26m −2, and 573 K. Transmission electron microscopy (TEM) samples were prepared using plasma-focused ion beam (FIB) followed by flash-polishing to effectively remove surface damages induced by FIB. The TEM images revealed that the general blisters observed on the exposed surface are associated with underlying cavities. A considerable amount of dislocations were found in the vicinity of the cavities. Prismatic dislocation loop arrays were observed, including small size 'coffee-bean' prismatic loops and large size prismatic loops. Near the tip of surfaces cavities, evidences for the emission of shear loops were also found. Based on the experimental findings, a multi-stage growth mechanism of H cavities was proposed. The loop-punching mechanism is operative for both very small cavities and cavities with sizes larger than several hundreds of nanometers. Whereas at intermediate sizes, cavities grow by emitting shear loops from the cavity tip.

AB - Due to a lack of direct experimental results, the detailed mechanisms that govern the blistering behavior of tungsten (W) exposed to ITER-relevant condition in nuclear fusion remain unclear. The growth mechanism of hydrogen (H) blisters is one example. In this work, recrystallized W was exposed to H plasma at 50 eV, 1.5×10 26m −2, and 573 K. Transmission electron microscopy (TEM) samples were prepared using plasma-focused ion beam (FIB) followed by flash-polishing to effectively remove surface damages induced by FIB. The TEM images revealed that the general blisters observed on the exposed surface are associated with underlying cavities. A considerable amount of dislocations were found in the vicinity of the cavities. Prismatic dislocation loop arrays were observed, including small size 'coffee-bean' prismatic loops and large size prismatic loops. Near the tip of surfaces cavities, evidences for the emission of shear loops were also found. Based on the experimental findings, a multi-stage growth mechanism of H cavities was proposed. The loop-punching mechanism is operative for both very small cavities and cavities with sizes larger than several hundreds of nanometers. Whereas at intermediate sizes, cavities grow by emitting shear loops from the cavity tip.

KW - Blistering behavior

KW - H plasma

KW - Loop punching

KW - Shear loop emission

KW - Tungsten

UR - http://www.scopus.com/inward/record.url?scp=85084477754&partnerID=8YFLogxK

U2 - 10.1016/j.actamat.2020.04.012

DO - 10.1016/j.actamat.2020.04.012

M3 - Article

VL - 193

SP - 19

EP - 27

JO - Acta Materialia

JF - Acta Materialia

SN - 1359-6454

ER -