Influence of sintering temperatures on hardness and Young's modulus of tricalcium phosphate bioceramic by nanoindentation technique

Changxiang Wang; X Zhou; M Wang

doi:10.1016/j.matchar.2004.06.007

Influence of sintering temperatures on hardness and Young's modulus of tricalcium phosphate bioceramic by nanoindentation technique

Changxiang Wang, X Zhou, M Wang

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Abstract

Nanoindentation experiments on tricalcium phosphate (TCP) bioceramic sintered at different temperatures were performed with a Berkovich indenter for determining hardness and elastic modulus from load and displacement data. The hardness and Young's modulus increased with the increase of sintering temperature up to 1300 degreesC, but the Young's modulus decreased with the further increase of sintering temperatures at 1400 and 1500 degreesC. X-ray diffraction (XRD) results showed that the transformation beta-->alpha-TCP happened when the sintering temperature reached around 1400 degreesC, which contributed to the decreases of modulus at 1400 and 1500 degreesC. Scanning electron microscopy (SEM) results showed that the sintering effect was improved with the increase in sintering temperature. (C) 2004 Elsevier Inc. All fights reserved.

Original language	English
Pages (from-to)	301-307
Number of pages	7
Journal	Materials Characterization
Volume	52
Issue number	4-5
DOIs	https://doi.org/10.1016/j.matchar.2004.06.007
Publication status	Published - 1 Jan 2004

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title = "Influence of sintering temperatures on hardness and Young's modulus of tricalcium phosphate bioceramic by nanoindentation technique",

abstract = "Nanoindentation experiments on tricalcium phosphate (TCP) bioceramic sintered at different temperatures were performed with a Berkovich indenter for determining hardness and elastic modulus from load and displacement data. The hardness and Young's modulus increased with the increase of sintering temperature up to 1300 degreesC, but the Young's modulus decreased with the further increase of sintering temperatures at 1400 and 1500 degreesC. X-ray diffraction (XRD) results showed that the transformation beta-->alpha-TCP happened when the sintering temperature reached around 1400 degreesC, which contributed to the decreases of modulus at 1400 and 1500 degreesC. Scanning electron microscopy (SEM) results showed that the sintering effect was improved with the increase in sintering temperature. (C) 2004 Elsevier Inc. All fights reserved.",

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T1 - Influence of sintering temperatures on hardness and Young's modulus of tricalcium phosphate bioceramic by nanoindentation technique

AU - Wang, Changxiang

AU - Zhou, X

AU - Wang, M

PY - 2004/1/1

Y1 - 2004/1/1

N2 - Nanoindentation experiments on tricalcium phosphate (TCP) bioceramic sintered at different temperatures were performed with a Berkovich indenter for determining hardness and elastic modulus from load and displacement data. The hardness and Young's modulus increased with the increase of sintering temperature up to 1300 degreesC, but the Young's modulus decreased with the further increase of sintering temperatures at 1400 and 1500 degreesC. X-ray diffraction (XRD) results showed that the transformation beta-->alpha-TCP happened when the sintering temperature reached around 1400 degreesC, which contributed to the decreases of modulus at 1400 and 1500 degreesC. Scanning electron microscopy (SEM) results showed that the sintering effect was improved with the increase in sintering temperature. (C) 2004 Elsevier Inc. All fights reserved.

AB - Nanoindentation experiments on tricalcium phosphate (TCP) bioceramic sintered at different temperatures were performed with a Berkovich indenter for determining hardness and elastic modulus from load and displacement data. The hardness and Young's modulus increased with the increase of sintering temperature up to 1300 degreesC, but the Young's modulus decreased with the further increase of sintering temperatures at 1400 and 1500 degreesC. X-ray diffraction (XRD) results showed that the transformation beta-->alpha-TCP happened when the sintering temperature reached around 1400 degreesC, which contributed to the decreases of modulus at 1400 and 1500 degreesC. Scanning electron microscopy (SEM) results showed that the sintering effect was improved with the increase in sintering temperature. (C) 2004 Elsevier Inc. All fights reserved.

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DO - 10.1016/j.matchar.2004.06.007

M3 - Article

SN - 1044-5803

VL - 52

SP - 301

EP - 307

JO - Materials Characterization

JF - Materials Characterization

IS - 4-5

ER -

Influence of sintering temperatures on hardness and Young's modulus of tricalcium phosphate bioceramic by nanoindentation technique

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