In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions

J. Solla-Gullón; F. J. Vidal-Iglesias; P. Rodríguez; E. Herrero; J. M. Feliu; J. Clavilier; A. Aldaz; Paramaconi Rodriguez

doi:10.1021/jp0471453

In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions

J. Solla-Gullón^*
, F. J. Vidal-Iglesias
, P. Rodríguez
, E. Herrero
, J. M. Feliu
, J. Clavilier
, A. Aldaz
, Paramaconi Rodriguez

^*Corresponding author for this work

Chemistry

Research output: Contribution to journal › Article › peer-review

95 Citations (Scopus)

Abstract

A new method for in situ surface characterization of preferentially oriented platinum nanoparticles is presented. The method is based on the use of structure-sensitive surface reactions such as the redox behavior of underpotential and spontaneous deposition of adatoms. Examples of its use for surface characterization of Pt nanoparticles synthesized by different methods are given. The method has been also employed to rationalize the different behavior of these Pt nanoparticles for the ammonia electro-oxidation in a basic medium.

Original language	English
Pages (from-to)	13573-13575
Number of pages	3
Journal	The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical
Volume	108
Issue number	36
DOIs	https://doi.org/10.1021/jp0471453
Publication status	Published - 9 Sept 2004

ASJC Scopus subject areas

Physical and Theoretical Chemistry

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Solla-Gullón, J., Vidal-Iglesias, F. J., Rodríguez, P., Herrero, E., Feliu, J. M., Clavilier, J., Aldaz, A., & Rodriguez, P. (2004). In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions. The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical, 108(36), 13573-13575. https://doi.org/10.1021/jp0471453

Solla-Gullón, J. ; Vidal-Iglesias, F. J. ; Rodríguez, P. et al. / In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions. In: The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical. 2004 ; Vol. 108, No. 36. pp. 13573-13575.

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abstract = "A new method for in situ surface characterization of preferentially oriented platinum nanoparticles is presented. The method is based on the use of structure-sensitive surface reactions such as the redox behavior of underpotential and spontaneous deposition of adatoms. Examples of its use for surface characterization of Pt nanoparticles synthesized by different methods are given. The method has been also employed to rationalize the different behavior of these Pt nanoparticles for the ammonia electro-oxidation in a basic medium.",

author = "J. Solla-Gull{\'o}n and Vidal-Iglesias, \{F. J.\} and P. Rodr{\'i}guez and E. Herrero and Feliu, \{J. M.\} and J. Clavilier and A. Aldaz and Paramaconi Rodriguez",

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Solla-Gullón, J, Vidal-Iglesias, FJ, Rodríguez, P, Herrero, E, Feliu, JM, Clavilier, J, Aldaz, A & Rodriguez, P 2004, 'In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions', The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical, vol. 108, no. 36, pp. 13573-13575. https://doi.org/10.1021/jp0471453

In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions. / Solla-Gullón, J.; Vidal-Iglesias, F. J.; Rodríguez, P. et al.
In: The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical, Vol. 108, No. 36, 09.09.2004, p. 13573-13575.

Research output: Contribution to journal › Article › peer-review

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AU - Solla-Gullón, J.

AU - Vidal-Iglesias, F. J.

AU - Rodríguez, P.

AU - Herrero, E.

AU - Feliu, J. M.

AU - Clavilier, J.

AU - Aldaz, A.

AU - Rodriguez, Paramaconi

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N2 - A new method for in situ surface characterization of preferentially oriented platinum nanoparticles is presented. The method is based on the use of structure-sensitive surface reactions such as the redox behavior of underpotential and spontaneous deposition of adatoms. Examples of its use for surface characterization of Pt nanoparticles synthesized by different methods are given. The method has been also employed to rationalize the different behavior of these Pt nanoparticles for the ammonia electro-oxidation in a basic medium.

AB - A new method for in situ surface characterization of preferentially oriented platinum nanoparticles is presented. The method is based on the use of structure-sensitive surface reactions such as the redox behavior of underpotential and spontaneous deposition of adatoms. Examples of its use for surface characterization of Pt nanoparticles synthesized by different methods are given. The method has been also employed to rationalize the different behavior of these Pt nanoparticles for the ammonia electro-oxidation in a basic medium.

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SN - 1520-6106

VL - 108

SP - 13573

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JO - The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical

JF - The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical

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Solla-Gullón J, Vidal-Iglesias FJ, Rodríguez P, Herrero E, Feliu JM, Clavilier J et al. In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions. The Journal of Physical Chemistry Part B: Condensed Matter, Materials, Surfaces, Interfaces & Biophysical. 2004 Sept 9;108(36):13573-13575. doi: 10.1021/jp0471453

In situ surface characterization of preferentially oriented platinum nanoparticles by using electrochemical structure sensitive adsorption reactions

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