Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes

JK Lee; MJ Fuchter; RM Williamson; Gary Leeke; EJ Bush; IF McConvey; S Saubern; JH Ryan; AB Holmes

doi:10.1039/b808374f

Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes

JK Lee, MJ Fuchter, RM Williamson, Gary Leeke, EJ Bush, IF McConvey, S Saubern, JH Ryan, AB Holmes

Chemical Engineering

Research output: Contribution to journal › Article

23 Citations (Scopus)

Abstract

A high yielding, batch mode synthesis of diaryl ethers and sulfides by an SNAr fluoride-mediated process in scCO(2) has been developed; the use of a polymer-supported imidazolium fluoride reagent in batch mode led to the development of a fixed-bed continuous flow process, with high conversions.

Original language	English
Pages (from-to)	4780-4782
Number of pages	3
Journal	Chemical Communications
Volume	n/a
Issue number	39
DOIs	https://doi.org/10.1039/b808374f
Publication status	Published - 1 Jan 2008

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10.1039/b808374f

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title = "Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes",

abstract = "A high yielding, batch mode synthesis of diaryl ethers and sulfides by an SNAr fluoride-mediated process in scCO(2) has been developed; the use of a polymer-supported imidazolium fluoride reagent in batch mode led to the development of a fixed-bed continuous flow process, with high conversions.",

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AU - Lee, JK

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AU - Williamson, RM

AU - Leeke, Gary

AU - Bush, EJ

AU - McConvey, IF

AU - Saubern, S

AU - Ryan, JH

AU - Holmes, AB

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AB - A high yielding, batch mode synthesis of diaryl ethers and sulfides by an SNAr fluoride-mediated process in scCO(2) has been developed; the use of a polymer-supported imidazolium fluoride reagent in batch mode led to the development of a fixed-bed continuous flow process, with high conversions.

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DO - 10.1039/b808374f

M3 - Article

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VL - n/a

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EP - 4782

JO - Chemical Communications

JF - Chemical Communications

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Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes

Abstract

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