3-({5-Bromo-4-[pyrrolidin-1-yl]pyrimidin-2-yl}amino)phenol

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Abstract

Re-investigation of the 1H-NMR spectrum reported for 15-bromo-4-oxa-2,9-diaza-1(2,4)-pyrimidine-3(1,3)-benzenacyclononaphane (2) prepared via a Mitsunobu- mediated macroether cyclisation led to a proposed structural isomer (3). The title compound (3) was prepared via a two-step protocol and assigned using 1H, 13C-NMR and LC-MS.
Original languageEnglish
Article numberM859
Number of pages4
JournalMolBank
Volume2015
Issue number2
DOIs
Publication statusPublished - 21 May 2015

Keywords

  • macrocyclic ether
  • Mitsunobu
  • macrocyclisation

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